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排序方式: 共有2112条查询结果,搜索用时 161 毫秒
11.
H. W. Brinks V. A. Yartys B. C. Hauback H. Fjellvg B. Ouladdiaf 《Journal of Alloys and Compounds》2002,340(1-2):62-66
TbNiSiD1.78 has been studied by powder neutron diffraction below 100 K. The compound takes the hexagonal room temperature structure at 100 and 50 K (P63/mmc). At 2 K, below the antiferromagnetic ordering temperature of 10 K, there is a small orthorhombic distortion of the lattice. The refined unit-cell dimensions at 2 K (space group Pnma) are a=7.9505(2), b=4.02502(14), c=6.9823(2) Å. The magnetic moments of Tb are 8.71(6) μB, and are ordered antiferromagnetically along a. 相似文献
12.
Hyun-Goo Kim Wha-Nam Myung K. Sumiyama K. Suzuki 《Journal of Alloys and Compounds》2002,340(1-2):270-274
We report upon the chemical leaching and magnetic properties of nanoscale crystalline Al0.6(Co25Cu75)0.4 alloy powders produced by rod milling. X-Ray diffractometry (XRD), transmission electron microscopy, differential scanning calorimetry, vibrating sample magnetometry, and superconducting quantum interference device magnetometry were used to characterize the as-milled and leached specimens. After 400 h of milling, only the b.c.c. phase of the intermetallic compound γ-Al3.892Cu6.10808 was detected by XRD. After annealing the leached specimen at 600 °C for 1 h, the nanoscale crystalline phase was transformed into the f.c.c. Cu phase, and this was accompanied by a change in the magnetic properties. The peaks of the magnetization shifted towards lower temperature with increasing external field. The temperature behavior at Tf (45 K) for direct current (d.c.) magnetic susceptibility measurements was quite different for field cooling and zero-field cooling. After cooling the leached specimen from 800 °C, magnetization increased gradually. 相似文献
13.
PowerPoint2000是Microsoft公司办公自动化软件Office2000的重要构件之一。其自身具有强大的处理功能,尤其是PowerPoint2000所提供的基本动画效果,更是给演示文稿增添了很多色彩。如果能将这些基本动画效果巧妙地组合在一起,就会创作出更富感染力的作品。就创作中的技巧并结合应用举例分析如下。相信人们可以利用这些设计思想,创作出更加精彩的作品。 相似文献
14.
15.
Bedich ika Helena Bendov Ivan Macha
《Chemical Engineering and Processing: Process Intensification》2005,44(12):1312-1319
A procedure has been proposed for the estimation of the terminal falling velocity of non-spherical particles moving in a Carreau model fluid in the transition flow region. The procedure is based on a modification of the relationship formerly developed for the fall of spherical particles including the particle dynamic shape factor. The suitability of the proposed procedure has been confirmed by good agreement between experimental and calculated terminal falling velocity data. In the experiments, the terminal falling velocity of short cylinders and rectangular prisms in polymer solutions of different measure of shear thinning and elasticity has been measured. 相似文献
16.
Maria Chiara Dalconi Giuseppe Cruciani Alberto Alberti Paolo Ciambelli 《Catalysis Today》2005,110(3-4):345-350
High-silica zeolites exchanged with transition metal ions (TMIs) are the subject of great interest for their unusual catalytic activity and selectivity. Structural information like coordination and accessibility of TMIs in zeolites are important factors for understanding their catalytic activity. Siting of TMIs in zeolites is typically obtained by spectroscopic (EXAFS, EPR, UV–vis and IR) and computational methods, as in the case of Co-ferrierite. However, some controversy exists in the literature concerning the model for incorporation of bare Co ions in ferrierite. We show here that the results of our synchrotron X-ray powder diffraction studies on Co- and Ni-exchanged ferrierite (Si/Al = 8.5) are in a good agreement with the model of Co siting based on an indirect spectroscopic approach and help to validate this model. By direct structural evidences, a possible explanation for the larger catalytic activity of Co sites in the main channels of ferrierite can be inferred. A combination of data from in situ XRD continuous monitoring of the Co ion migration during calcination and crystal-chemical considerations allows to device a strategy for the design of optimised co-cations containing Co-ferrierite catalysts. 相似文献
17.
Mgidi Donald Dlamini 《Solar Energy Materials & Solar Cells》1996,43(4):353
In this paper results on surface photovoltage (SPV) and electron beam induced conductivity (EBIC) studies of edge-defined film-fed growth (EFG) and floating zone (FZ) silicon solar cell materials (both p-type) are presented. A systematic comparison based on minority carrier diffusion length and carrier recombination is made between: (i) samples contaminated with Ti and/or Fe, (ii) samples gettered by phosphorous diffusion, and (iii) as-received samples. Deep level transient spectroscopy (DLTS) measurements, together with the iron-boron (FeB) pairing kinetics [1] have successfully been used to detect the presence of Fe in the samples. Even though this process is effective in revealing Fe impurities in p-type FZ silicon it is evidently not suitable for Fe identification in p-type EFG silicon. Ti, like Fe, is found to be a prominent lifetime-limiting metallic impurity in both EFG and FZ silicon. Phosphorous diffusion is proven to be an effective external gettering technique for fast-diffusing impurities such as Fe, but not for Ti. 相似文献
18.
介绍了间接跃迁的半导体AlP与GaP形成的超晶格,由于零折叠效应,实现了能带由间接带隙向直接带隙的转变,从而增加了带间的光跃迁几率,并推导了该几率的表达式。 相似文献
19.
A. Andreev L. Prahov M. Gabrovska A. Eliyas V. Ivanova 《Applied catalysis. B, Environmental》1996,8(4):365-373
The catalytic activity of a wide range of transition metal oxides in oxidation of sulphide ions by air in aqueous medium was studied. Some specific features of the reaction mechanism on some of the studied oxides were considered. The transition metal oxides are promising catalysts for practical application. Some of these oxides will allow the preparation of catalysts possessing activity comparable to that of the cobalt phthalocyanine based catalysts, popular in industrial practice. 相似文献
20.
HPAM/柠檬酸铝胶态分散凝胶形成条件研究 总被引:41,自引:7,他引:34
采用一种简化的实验程序测定胶态分散凝胶(CDG)的转变压,用测得的转变压值作为评价参数,考察由HPAM、柠檬酸铝、硫脲、氯化钾组成的CDG的形成条件及相对强度。所考察的形成条件包括HPAM的来源和浓度,柠檬酸铝和氯化钾的浓度,pH值,绝大部分实验工作在40℃和pH=7.0的条件下进行,用一组实验考察了温度的影响(70℃和40℃)。 相似文献